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This article is the fourth part of a series of “anatomy” lessons within Machinery Lubrication. In this issue, the various modes by which wear debris is created will be examined along with the physical characteristics of each type of wear particle. In addition, microscopic analysis and similar instrumentation will be used to provide an in-depth look at these particles’ unique appearances and how they are formed.
Mechanical equipment deteriorates over time. Depending on the type of work and environmental conditions a machine endures, internal mechanical deterioration can occur in the form of fatigue, rubbing, sliding, abrasion and corrosion. From a macroscopic perspective, the wear debris produced from these deterioration processes may appear as insignificant specks of mass that mostly act and look the same. However, on a microscopic level, this wear debris has a unique morphology (shape and size) and surface topography (roughness, texture and surface pattern) based on the deterioration process or wear mode by which it was produced. If clearly understood, the morphology and topography can offer clues that can be used to prevent imminent machine failure.
Wear debris can be defined as particles produced from the breakdown of surfaces within a machine. These particles can range from a submicron size to chunks of metal as large as can be imagined. Wear debris analysis generally focuses on the small, destructive particles, many of which are too small for the human eye to see. These particles may be less than 1 micron to 200 microns in size. If you have particles larger than 200 microns, you probably don’t need anyone to tell you that there is a serious issue within the machine.
There are many wear debris analysis techniques (see Table 1). Some of these methods can even analyze wear debris right from the oil sample. Analytical ferrography requires wear debris to first be isolated from the collected oil sample. Photomicrograph images of the ferrograms or filtergrams are then studied using an optical microscope. The main advantage of analytical ferrography is its ability to determine particle shapes, sizes and textures as well as identify elements.
Ferrography utilizes either magnetism or membrane filtration to collect particles. ISO standards, such as ISO 16232, ASTM D7670 and D7690, are used to properly prepare these samples and analyze the particles’ visual characteristics. These observed characteristics shed light on where and how these particles were generated.
In this ferrogram, ferrous particles are
aligned along magnetic fields.
As an oil sample flows down a specially designed glass slide called a ferrogram, a magnet is positioned underneath to trap the ferrous particles. The particles tend to collect in strings along the magnetic field. While many of the non-ferrous particles will flow past and not become trapped, some will be held up by gravity or by contact with the trapped ferrous particles. Both bottom and top lighting can be used to help characterize the particles’ critical features.
Particles collect at random
on a filtergram.
In contrast with ferrograms, filtergrams do not have any bias toward ferrous particles. As the oil sample is forced through a filter membrane, any particles greater than the pore size are randomly trapped on the membrane surface. However, bottom light transmission during analysis is poor due to the opaqueness of the filter membrane.
As the most common type of wear, rubbing wear occurs whenever there is surface sliding contact within a machine. During initial surface contact, this type of “break-in” wear should be expected. It usually results in a smoother, low-wearing surface. Particles produced from rubbing wear typically have a platelet (two-dimensional) morphology and smooth topography.
This abnormal wear is produced when two surfaces penetrate one another. As its name suggests, particles are generated from one surface gouging the other surface, creating long, ribbon-like chunks. This wear mode is often compared to machining swarf from a lathe but on a much smaller scale.
Rolling surface contact produces surface fatigue. Particles generated from surface fatigue tend to come in the form of spalls, spherical or laminar particles. The formation of pits and spalls as a result of high load and a low-contact surface area leads to the shaping and sizing of these particles as they are forced out of their original setting. This type of wear typically occurs with components of rolling motion contact, such as in the case of ball bearings.
This abnormal combination of wear modes is caused by fatigue and scuffing. It is commonly associated with gear systems, particularly along the pitchline of gear teeth as well as in conditions with too high of a load or speed and excessive heat generation. For example, the surface contact of gear teeth is a combination of rolling and sliding motion. This combined wear mode region, along with the effects of lubricant contaminants, can generate a complex fusion of wear debris.
A severe level of wear occurs in excessive loads and high speeds between contacting surfaces. When surface stresses are too great because of increased load and/or speed on the surface contact area, the area becomes unstable and large particles break away, further increasing the wear rate.
Corrosive wear is frequently labeled as fretting corrosion, erosion, stress fatigue, etc. These particles are often too small to distinguish individually and are usually the result of improper fluid properties or heavy contamination from water, acid, salt or bacteria. Heat also plays a major role in corrosion. Most lubricants have rust/corrosion-inhibiting additives to combat the effects of chemical wear.
Since wear particles detach from internal machine surfaces in a variable manner, their morphology and topography are unique. However, they also fit certain patterns based on the actions by which they become detached.
These two-dimensional particles are generally flat with a rough perimeter. Their thickness typically is about one-tenth to one-thirtieth their lateral dimension. They can be further described as having either a laminar or wedge shape. One of the most common ways platelet-shaped particles can occur is by normal and tangential forces through contacting asperities.
As their name implies, these particles are fundamentally spherical. Normally less than 10 microns, they appear in small numbers and are sometimes fused together. As wear debris, spherical particles have been associated with rolling-element bearings and are often a precursor to fatigue failure. It must be noted that spherical particles are frequently found as contaminants rather than as wear debris. This type of spherical-shaped contaminant likely will be larger than 10 microns and often is a byproduct of welding and grinding processes.
Typically long and skinny, these particles may resemble a wire, splinter or ribbon shape. While they can have smooth sides and edges, they normally will have a rougher appearance. Another common characteristic is how they are curled, which is similar to a shaving curl in a wood-planing process. For this reason, the particle may be rough on one side and smooth on the other. These types of particles have been linked to cutting wear where one of the contacting surfaces possesses an asperity or lodged particle that is plastically rigid compared to the other surface from which the ribbon-shaped particle is gouged out.
The adhesion theory offers a possible explanation for why particles produce irregular shapes. During surface adhesion, the asperities of two contacting surfaces flatten each other, creating a fracture on one of the surfaces. The surface interaction transfers fragment material, which adheres to the opposing surface. This can result in the formation of particles that have unusual shapes and are a mixture of elements. The shapes often are difficult to define, as several wear modes may be at work concurrently within the system. As these wear particles act as abrasive contaminants between continually contacting surfaces, they transform into unusual shapes.
Corrosion particles typically are extremely small (submicron). Magnetic collection techniques can be effective in gathering these particles, which are too small to view in individual detail.
Oxide particles, which are either red or black iron oxides, are produced from chemical reactions between iron and oxygen. Red oxides are an indication of moisture in the system, while black oxides indicate inadequate lubrication and excessive heat generation in the system.
The particles described previously comprise only those generated from wear-induced causes, but a mechanical system can contain an assortment of other particles from environmental contaminants like water, dust, etc., to human-agency contaminants such as machining byproducts. Even some lubricant additives can be mistaken for wear particles during wear debris analysis. Nevertheless, wear debris analysis is quite useful for discovering which degrading actions are occurring within a machine or how a machine failed.
This illustration shows how the various types of wear particles are associated with the different wear modes.
Although analysis techniques such as observations from precise heat treatments or adding specific chemicals can help in determining the elemental composition of particles, spectrometric analysis is generally more effective in providing the elemental composition of contaminants within an oil sample. Analytical ferrography remains the best technique for determining the morphology and topography of wear debris, which is essential in identifying the root cause of the particles.
Anderson, Dan P. (2012). Wear Debris Atlas. Jim C. Fitch (Technical Editor). Tulsa, OK: Noria Corporation.
Rigney, David A. (1981). Fundamentals of Friction and Wear of Materials. Metals Park, OH: American Society for Metals.
Thibault, Ray. (2006, Nov.-Dec.). “Improving Predictive Maintenance Through Wear Debris Analysis.” Lubrication & Fluid Power.